Chem 12B
Safety Information
Safety in Academic Chemical Laboratories
www.msds.com (list of all MSDS from all companies)
MSDS at Fisher Scientific (an equipment and chemical supplier)
Organic Laboratory Safety Rules
Experiments
IR Workshop – Identification of Spectra. Second Semester
NMR experiment (Klein Pavia) S20 v2
NMR experiment (Klein Pavia) Worksheet S20
Dehydration of 2-methylcyclohexanol
Dehydration Mixture from Experiment 24A, S20
Resolution of Racemic α-Phenylethylamine (aka, α-Methylbenzylamine)
Resolution of α-Phenylethylamine (Org. Syn. Procedure)
SR-6 Polarimeter Instruction Manual
Preparation_of_N-benzoyl-α-phenylethylamine
Oxone Technical Bulletin (Dupont)
An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol. Prelab Exercise
An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol. Week 1, S20
An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol. Week 2, S20
Triphenylmethanol (Grignard lab), S20
Methyl Salicylate (Oil of Wintergreen), S20
Methyl Salicylate procedure (old-Pavia), S20
The Diels-Alder Reaction. Preparation of cis-norbornene-5,6-endo-dicarboxylic anhydride
Molecular Modeling and Mechanics – Endo vs. Exo Diels-Alder Product, S20
Spectrometer Guides
IR Instructions – KBr pellets S20
1H NMR Instructions – Simple (proton), S20
13C NMR Instructions – Simple (carbon), S20
1H 1D Spectrum Guide (modified)
13C 1D Spectrum Guide (modified)
Reference
Guide to References – ACS Style guide
Guide to Abstracts – ACS Style guide
Separation Scheme Tips and Notes
Lab Report Guidelines and Checklist, Spring 2020
Spectroscopy Reference
Online NMR Resources, Spring 2018
MIRacleATR User Manual (ATR IR)