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Laney College

Laboratory

Laboratory

Chem 12B

Safety Information

Safety in Academic Chemical Laboratories

www.msds.com  (list of all MSDS from all companies)

MSDS at Fisher Scientific (an equipment and chemical supplier)

Organic Laboratory Safety Rules

Experiments for Fall 2019

IR Workshop – Identification of Spectra. Second Semester

Dehydration of 2-methylcyclohexanol

Resolution of Racemic α-Phenylethylamine (aka, α-Methylbenzylamine)

Resolution of α-Phenylethylamine (Org. Syn. Procedure)

SR-6 Polarimeter Instruction Manual

Preparation_of_N-benzoyl-α-phenylethylamine

Resolution Data, F19

Extraction of Essential Oils from Caraway, Cinnamon, Cloves, Cumin, Fennel, or Star Anise by Steam Distillation, F19

Oxone Technical Bulletin (Dupont)

An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol. Prelab Exercise

An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol. Week 1, F19

An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol. Week 2, F19

Methyl Salicylate (Oil of Wintergreen), F19

Methyl Salicylate procedure (old-Pavia), F19

The Diels-Alder Reaction. Preparation of cis-norbornene-5,6-endo-dicarboxylic anhydride

Diels-Alder adduct spectral data Fall 2019

Molecular Modeling and Mechanics – Endo vs. Exo Diels-Alder Product, F19

Synthesis of Acetylferrocene, F19

Old Experiments

Nuclear Magnetic Resonance (NMR). Identification of an Unknown Substance.

Grignard Reaction:  Synthesis of Triphenylmethanol

Grignard Reaction:  Triphenylmethanol Spectroscopy Data

Old Experiments

Identification of a Natural Product. A Spectroscopy Experiment.

Anazasi NMR Spectrometer Guides

1H 1D Spectrum Guide (modified)

13C 1D Spectrum Guide (modified)

DEPT Spectrum Guide

COSY Spectrum Guide

HETCOR Spectrum Guide

Reference

Abstract Guidelines

Separation Scheme Tips and Notes

Lab Report Guidelines and Checklist, Fall 2019

Spectroscopy Reference

Sample IR Websites

Online NMR Resources, Spring 2018

Reich NMR site (advanced)

MIRacleATR User Manual (ATR IR)