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Laney College

Laboratory

Laboratory

Chem 12B

Safety Information

Safety in Academic Chemical Laboratories

www.msds.com  (list of all MSDS from all companies)

MSDS at Fisher Scientific (an equipment and chemical supplier)

Organic Laboratory Safety Rules

Experiments for Spring 2020

IR Workshop – Identification of Spectra. Second Semester

NMR experiment (Klein Pavia) S20 v2

NMR experiment (Klein Pavia) Worksheet S20

Dehydration of 2-methylcyclohexanol

Dehydration Mixture from Experiment 24A, S20

Resolution of Racemic α-Phenylethylamine (aka, α-Methylbenzylamine)

Resolution of α-Phenylethylamine (Org. Syn. Procedure)

SR-6 Polarimeter Instruction Manual

Preparation_of_N-benzoyl-α-phenylethylamine

Extraction of Essential Oils from Caraway, Cinnamon, Cloves, Cumin, Fennel, or Star Anise by Steam Distillation, S20

 

Oxone Technical Bulletin (Dupont)

An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol. Prelab Exercise

An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol. Week 1, S20

An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol. Week 2, S20

Methyl Salicylate (Oil of Wintergreen), S20

Methyl Salicylate procedure (old-Pavia), S20

The Diels-Alder Reaction. Preparation of cis-norbornene-5,6-endo-dicarboxylic anhydride

Molecular Modeling and Mechanics – Endo vs. Exo Diels-Alder Product, S20

Spectrometer Guides

IR Instructions – KBr pellets S20

1H NMR Instructions – Simple (proton), S20

13C NMR Instructions – Simple (carbon), S20

1H 1D Spectrum Guide (modified)

13C 1D Spectrum Guide (modified)

DEPT Spectrum Guide

COSY Spectrum Guide

HETCOR Spectrum Guide

Reference

Guide to References – ACS Style guide

Guide to Abstracts – ACS Style guide

Separation Scheme Tips and Notes

Lab Report Guidelines and Checklist, Spring 2020

Spectroscopy Reference

Sample IR Websites

Online NMR Resources, Spring 2018

Reich NMR site (advanced)

MIRacleATR User Manual (ATR IR)