Tuesday, 3/29 Complete separation of a mixture Thursday, 3/31 No Lab–Cesar Chavez Holiday
Tuesday, 3/29 Complete separation of a mixture Thursday, 3/31 No Lab–Cesar Chavez Holiday
Monday, March 28 Start Biodiesel Experiment (Pavia 27 A and C) Acquire an IR spectrum and 1H NMR Submit Sample for GC-MS analysis Formal Report Wednesday, March 30 Complete Biodiesel Experiment Submit Partial Reports for Diels-Alder (mandatory solo) and Nitration of Aromatic Compounds (joint report acceptable) Wednesday March 30 and Thursday, March 31 Quiz 4: […]
Monday, March 14 Complete Nitration Experiment Grignard Formal Report Due Wednesday, March 16 Reactivities of Aromatic Compounds (Pavia 40) Prelab Quiz Substrates will be assigned on Monday
Tuesday, March 15 Lab Lecture on Distillation and Gas Chromatography Collect GC Data Submit draft separation scheme for Pavia 5 (see prelab guidelines) Thursday, March 17 Separation of a Mixture (Pavia 5) Chromatography Template Report Due Tuesday, March 31 Distillation Partial Report Due
Tuesday, March 8 Chromatography (Pavia 6D) There will be a prelab quiz And a prelab lecture See prelab guidelines Thursday, March 10 Simple and Fractional Distillation (Pavia 7 A and B) There will be a prelab quiz Guidelines are forthcoming
Monday March 7 Diels-Alder Reaction (Pavia 47 with a significant change in procedure on prelab guidelines) Wednesday, March 9 Start Nitration of Aromatic Compounds (Pavia 29) Wednesday March 9 and Thursday March 10 Lecture Quiz Diels Alder Reaction
Monday, February 29 Grignard Experiment (Pavia33) See prelab guidelines You will first prepare the reagent (pg. 308-309) …and react with benzophenone (Part A) Wednesday, March 2 Complete Grignard experiment Due: Partial Report for Oxidation-Reduction Scheme See additional guidelines No joint reports
Tuesday, March 1 Isolation of Caffeine from Tea (Pavia 13A) See prelab guidelines Report will be combined with the Extraction Experiment template report Due: Template Report for Crystallization Thursday, March 3 Exam 1 No reports due
Monday, 2/22 Finish Reduction of Camphor You will need the following for your report: Melting points of camphor and isoborneol IR spectra for camphor and isoborneol GC-MS data for reduction product Wednesday, 2/24 Exam 1 See prospectus and sample exams on 12B Exam Preparation page
Tuesday, 2/23 Crystallization (Pavia 3C) Pay careful attention to the prelab guidelines There is a prelab calculation that must appear in your notebook You will performing Part C, but will have to reply heavily on the procedure given in Part A and Technique 111.6 BP/IR template report due Thursday, 2/25 Extraction Pavia 4A and 4D […]